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CAS № 77-71-4Имя:5.5-диметилгидантоиновогоСинонимы:T10DMHt10[qr]дмх[qr]нск8652дантоиндмхдмгидантоинD...
CAS № 77-71-4
5.5-диметилгидантоинового
T10
DMH
t10[qr]
дмх[qr]
нск8652
дантоиндмх
дмгидантоин
DM Гидантоин
Диметилгидантоин
5.5-диметилгидантоинового
5.5-Диметилгидрантоин
5.5-Диметилгидантоин
Гидантоин, 5.5-диметил-
5.5-диметил-2.4-имидазолидиндион
5.5-диметилимидазолидин-2.4-дион
5. 5-dimethylhydantoin is an important organic synthesis intermediate with a wide range of uses, it is a heterocyclic compound with a certain rigid skeleton. A range of valuable derivatives can be prepared by substitution reactions. Such as: dibromohydantoin, dichlorohydantoin and other widely used in organic synthesis, medicine, plastics, food, cosmetics, pesticides and other production areas.
5. 5-dimethylhydantoin, also known as 5. 5-dimethylhydantoin, DMH, is a wide range of uses of organic synthesis intermediates, is a rigid heterocyclic compounds, can be prepared by substitution reaction of a series of valuable derivatives, such as: dibromohydantoin, dichlorohydantoin and other widely used in medicine, fine Chemicals in the production of pesticides, plastics and cosmetics.
preparation a. Add 600-800 parts of ammonium bicarbonate and 500-700 parts of acetone cyanohydrin to water and stir to fully dissolve, sealed when heated to 10 ℃; B. 30-50 parts of ammonia gas is introduced into the material prepared by Step a, and heated slowly to 50-65 ℃ for 1-2 hours, and stirring; c, the material prepared by Step B is heated to 75~85 ℃, the air is drawn for 30~50 minutes, and then cooled to room temperature and filtered to obtain crude dimethyl hydantoin and mother liquor; d. 950~1150 parts of crude dimethyl hydantoin prepared by Step c is put into a mixture of 150~300 parts of water and 700~900 parts of mother liquor, after heating to 80~98 ° C., 3~8 parts of activated carbon is added, decolorization is carried out for 20~40 minutes, the activated carbon is removed by filtration, and then crystallization is cooled, centrifugal filtration and drying are carried out to obtain a dimethyl hydantoin finished product.
for amino acid synthesis, but also as a special epoxy resin and water-soluble resin, fungicides, preservatives, etc. Its derivatives such as 1. 3-dichloro-5. 5-dimethylhydantoin can be used as chlorinating agent, Disinfection bactericide, 3-hydroxymethyl-5. 5-dimethylhydantoin is useful as a formaldehyde agent, a preservative, and the like.
mainly used as disinfectant, epoxy resin and amino acid raw materials
is obtained by reacting acetone cyanohydrin ([75-86-5]) with an aqueous ammonium carbonate solution at 50-80 °c.
Атрибут | Подробнее |
---|---|
Химическое название | 5.5-диметилгидантоинового |
Другие названия | 5.5-Dimethyl-2.4-imidazolidinedione; 5.5-Dimethylimidazolidine-2.4-dione; Dimethylhydantoin; etc. |
Номер по CAS | 77-71-4 |
Молекулярная формула | C5H8N2O2 |
Молекулярная масса | X |
Внешний вид | White to grayish white crystals or crystalline powder |
Температура плавления | 175°C (literature value may vary slightly) |
Плотность | 1.142 g / cm³ |
Точка возгорания | 193 ° C |
Растворимость | Soluble in water, ethanol, ethyl acetate, and dimethyl ether; slightly soluble in isopropanol, acetone, and methyl ethyl ketone; insoluble in aliphatic hydrocarbons and trichloroethylene |
Способ производства | Obtained by reacting acetone cyanohydrin with ammonium carbonate aqueous solution at 50-80°C |
Приложения | Used in amino acid synthesis; as a specialty epoxy resin and water-soluble resin; as a fungicide and preservative; derivatives such as 1.3-dichloro-5.5-dimethylhydantoin are used as chlorinating agents and disinfectants, while 3-hydroxymethyl-5.5-dimethylhydantoin is used as a formaldehyde agent and preservative |
Условия хранения | Store in a cool, dry place, away from direct sunlight and heat, and keep away from incompatible materials |
Информация по технике безопасности | Handle with caution, avoiding contact with skin and eyes; follow standard chemical safety procedures and wear appropriate protective clothing and eye/face protection |
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